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Title Monolithic silicas in separation science : concepts, syntheses, characterization, modeling and applications / edited by Klaus K. Unger, Nobuo Tanaka, and Egidijus Machtejevas.
Imprint Weinheim : Wiley-VCH, 2011.


 Internet  Electronic Book    AVAILABLE
Description 1 online resource (xviii, 344 pages)
Bibliog. Includes bibliographical references and index.
Note Available only to authorized UTEP users.
Print version record.
Subject Silicon -- Separation.
Contents Monolithic Silicas in Separation Science; Contents; Preface; List of Contributors; 1: The Basic Idea and the Drivers; 1.1: Definitions; 1.2: Monoliths as Heterogeneous Catalysts; 1.3: Monoliths in Chromatographic Separations; 1.4: Conclusion and Perspectives; References; Part One: Preparation; 2: Synthesis Concepts and Preparation of Silica Monoliths; 3: Preparation and Properties of Various Types of Monolithic Silica Stationary Phases for Reversed-Phase, Hydrophilic Interaction, and Ion-Exchange Chromatography Based on Polymer-Coated Materials; Part Two: Characterization and Modeling.
4: Characterization of the Pore Structure of Monolithic Silicas5: Microscopic Characterizations; 6: Modeling Chromatographic Band Broadening in Monolithic Columns; 7: Comparison of the Performance of Particle-Packed and Monolithic Columns in High-Performance Liquid Chromatography; 7.1: Introduction; 7.2: Basic Columns Properties; 7.3: Comparison of the Through-Pore Structures and Related Properties; 7.4: Thermodynamic Properties; 7.5: Kinetic Properties and Column Efficiency; 7.6: Conclusions; Part Three: Applications.
8: Quantitative Structure-Retention Relationships in Studies of Monolithic Materials9: Performance of Silica Monoliths for Basic Compounds. Silanol Activity; 10: Quality Control of Drugs; 11: Monolithic Stationary Phases for Fast Ion Chromatography; 12: Monolithic Chiral Stationary Phases for Liquid-Phase Enantioseparation Techniques; 13: High-Speed and High-Efficiency Separations by Utilizing Monolithic Silica Capillary Columns; 14: Silica Monolithic Columns and Mass Spectrometry; 15: Silica Monoliths for Small-Scale Purification of Drug-Discovery Compounds.
16: Monolithic Silica Columns in Multidimensional LC-MS for Proteomics and Peptidomics17: Silica Monoliths in Solid-Phase Extraction and Solid-Phase Microextraction; 17.1: Introduction; 17.2: Extraction Process; 17.3: Extraction Platforms; 17.4: Applications; 17.5: Conclusion and Outlook; References; Index.
Summary Edited by the experts and pioneers in the field, this is the first monograph to cover the topic, containing the must-have information hitherto only scattered among journals. Clearly divided into sections on preparation, characterization and modeling, and applications, this is essential reading for chemists, chromatographers, analytical chemists, biochemists and biologists.
Other Author Unger, Klaus K.
Tanaka, Nobuo.
Machtejevas, Egidijus.
Other Title Print version: Unger, Klaus K. Monolithic Silicas in Separation Science. Weinheim : Wiley-VCH, 2011 9783527633258